【摘要】 采用阳极氧化法成功制备出整体多通道Fe-Fe₂O₃,并以整体多通道Fe-Fe₂O₃为阴极,铂片为阳极,外加H₂O₂,构建非均相芬顿体系,利用电催化作用促进Fe（Ⅲ）还原为Fe（Ⅱ）.结果显示:在溶液pH为7,H₂O₂浓度为1.0 mmol/L,施加电压为-0.4 V的条件下,苯酚去除率在60 min内能够达到96%,这表明整体多通道Fe-Fe₂O₃是较理想的非均相催化剂.ICP溶出测试结果说明,电催化作用能够有效促进Fe（Ⅲ）还原为Fe（Ⅱ）,从而提高催化效率.更多还原

【Abstract】 The Fe-Fe₂O₃ monolith is successfully prepared by anodization method. Fe-Fe₂O₃ monolith and Pt sheet are employed as the cathode and anode, respectively, and H₂O₂ is added externally to construct the heterogeneous Fenton system. Meanwhile, the Fe（Ⅲ） is reduced to Fe（Ⅱ） by electrocatalysis. It is found that the phenol removal rate can reach 96% in 60 min under the condition in which pH is 7, H₂O₂ concentration is 1.0 mmol/L and applied voltage is-0.4 V. The result shows that Fe-Fe₂O₃ monolith is an ideal heterogeneous catalyst. The results of ICP test show that electrocatalysis can effectively promote the reduction of Fe（Ⅲ） to Fe（Ⅱ）, thereby improve catalytic efficiency.更多还原