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香菇中亚硫酸盐的离子色谱法测定

The Measurement of Sulfite in Lentinus Edodes by Ion Chromatography

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【作者】 姜川邹小龙田晓宇

【Author】 JIANG Chuan,ZOU Xiaolong,TIAN Xiaoyu (Lishui Municipal Institute of Quality and Technical Supervision and Testing,Lishui 323000,Zhejiang)

【机构】 丽水市质量技术监督检测院

【摘要】 建立了香菇中亚硫酸盐的离子色谱检测方法。样品经过超纯水浸提后,过滤进样分析。选用IonPac As19型分离柱,4mmol/LNaOH为淋洗液。此方法的线性相关性好,相关系数为0.9994,相对标准偏差为0.9%~2.1%,样品的加标回收率在97.0%~102.0%之间。

【Abstract】 A method for the determination of sulfite in lentinus edodes by ion chromatography is established.Ionpac As19 is chosen as the separation column and 4mmol/L NaOH as eluent.After digestion using deionized water and filtration with 0.45μm pinhead percolator,the samples are injected and analyzed.It is indicated that this method has a good relativity(r=0.9994).The relative standard deviations and recoveries are 0.9%~2.1% and 97.0%~102.0%,respectively.The method is proved to be rapid,accurate and practical.

  • 【文献出处】 丽水学院学报 ,Journal of Lishui University , 编辑部邮箱 ,2012年05期
  • 【分类号】TS219;O657.75
  • 【被引频次】2
  • 【下载频次】55
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